Xl. Tan et al., LOADING MODE DEPENDENCE OF DEFORMATION MICROSTRUCTURE IN A HIGH-PURITY TITANIUM SINGLE-CRYSTAL ORIENTED FOR DIFFICULT GLIDE, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 189(1-2), 1994, pp. 77-84
A special high-purity titanium single crystal was prepared to study th
e effect of loading mode on deformation microstructure. Six rectangula
rly sectioned specimens were cut from the same single crystal. The loa
ding axis of the specimens was parallel to the C-axis of the crystal,
and the wide surface was parallel to the prism plane {1010}, with the
narrow surface {1210}. Mechanical tests were conducted within the cham
ber of a scanning electron microscope JSM35C using a specially designe
d apparatus with closed-loop computer control. Five loading modes were
used: monotonic tension, tension-tension fatigue, and tension-compres
sion fatigue with three different stress amplitudes. The surface appea
rance of the specimens was registered with SEM periodically, and the c
yclic twins as well as persistent slip bands were identified using tra
ce analysis technique. The substructures of the tested specimens were
examined with a transmission electron microscope on foils cut from the
specimens parallel to the wide surface. The dislocation structures of
specimens tested in different modes were observed, and the slip syste
ms and twinning modes for each case are discussed.