Ab. Pandey et al., HIGH-TEMPERATURE CREEP OF AL-TIB2 PARTICULATE COMPOSITES, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 189(1-2), 1994, pp. 95-104
Two Al-20vol.%TiB2 composites produced by different processing routes,
namely conventional powder metallurgy (PM) and XD(TM) (XD(TM) is a pr
oprietary process of Martin Marietta Laboratories), were creep tested
under compression in the temperature range 573-673 K to evaluate the s
teady state creep mechanisms. The steady state creep rate data of the
conventional composite, covering almost five orders of magnitude in cr
eep rate, were rationalized in terms of the substructure invariant mod
el, which predicts a stress exponent of eight and lattice diffusion co
ntrol, together with the existence of a threshold stress. The higher v
alues of the apparent stress exponent (8-14) and the apparent activati
on energy (339 kJ mol(-1)), observed for the XD composite, do not agre
e with the existing models for dislocation creep even after considerin
g the threshold stress. This is possibly because of the anomalous cree
p behaviour of the XD composite observed at higher temperatures. A com
parison of the steady state creep data for PM Al-TiB2 and Al-SiC compo
sites shows that the SiC particulate provides better creep resistance
than the TiB2 particulate. The XD Al-TiB2 composite has better creep s
trength than the conventional Al-TiB2 composite; however, its creep st
rength is inferior to the Al-SiC composite. It has been suggested that
an applied stress-independent load transfer mechanism is required to
explain the origin of the threshold stress for steady state creep in d
iscontinuously reinforced Al matrix composites.