For the transient heat conduction of a thin slab, the temperature-time
history of its mid-point can be determined from a plane wall theory,
provided that a slab thickness to length ratio of 0.2 or smaller is us
ed in the experiments. Using the theory, two data reduction methods ar
e described for deducing the thermal properties of conductivity (k) an
d diffusivity (alpha) simultaneously from a single transient heating e
xperiment. The first method uses an analytical technique to fit the in
flection point on the temperature-square root(t) history plot to the t
heoretical inflection point. The second method, which was earlier prop
osed by the authors, uses a statistical curve fitting procedure to obt
ain the best fit between theory and experiment over seven points on th
e temperature-time history. Comparisons of the k values obtained by th
ese methods against steady-state heat conduction measurements of the s
ame slabs for various building construction materials indicate good ag
reement, and give support to the validity of these procedures. The val
ues of k and alpha obtained by these procedures also compare favourabl
y with reported literature data.