The authors report C-13, Rb-87, K-39, and Cs-133 nuclear magnetic reso
nance (NMR) measurements of lineshapes, Knight shifts, and spin-lattic
e relaxation rates in the normal and superconducting states of M(3)C(6
0), where M(3) = Rb-3, K-3, Rb2K, RbK2, Rb2Cs, and RbCs2. Measurements
are used as a guide to a new ammonia solvent synthesis technique. Tem
perature dependence of the superconducting state electron spin suscept
ibility is found to follow BCS weak coupling predictions. The issue of
the Hebel-Slichter coherence peak is addressed.