A C-60-DERIVATIZED DIPEPTIDE

Authors
WANG NX LI JS ZHU DB CHAN TH
Citation
Nx. Wang et al., A C-60-DERIVATIZED DIPEPTIDE, Tetrahedron letters, 36(3), 1995, pp. 431-434
Citations number
19
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Tetrahedron letters → ACNP
ISSN journal
00404039
Volume
36
Issue
3
Year of publication
1995
Pages
431 - 434
Database
ISI
SICI code
0040-4039(1995)36:3<431:ACD>2.0.ZU;2-R
Abstract
Methyl glycylglycinate(aqueous) reacted with C-60 in chlorobenzene at 110-120 degrees C by adding a few drops of bromine in 2mL of 2N NaOH a nd 0.6g of tetrabutylammonium chloride (phase transfer catalyst) to fo rm the adduct compound. The product was-isolated by column chromatogra phy and identified by FD-MS, UV-Vis, IR, H-1 NMR, C-13 NMR to be a C-6 0-derivatized Dipeptide.