H. Maruyama et al., FERROMAGNETIC-RESONANCE IN NI FILMS PRODUCED BY BIASED DC SPUTTER-DEPOSITION ONTO SIO2 AND SI(100), Thin solid films, 254(1-2), 1995, pp. 224-228
Ferromagnetic resonance measurements at the X-band were taken at room
temperature mainly to investigate the mechanical properties of Ni film
s 180 nm thick prepared on both pure and SiO2-covered Si(100) substrat
es at 190 degrees C by biased d.c. plasma sputter deposition at 2.5 kV
in Ar gas. A negative bias voltage V-s between 0 V and -80 V was appl
ied to the substrates during deposition. The homogeneous intrinsic str
ess sigma(i) induced in the films is compressive (sigma(i) < 0). The m
agnitude of sigma(i) depends on V-s. For the Ni/SiO2 system -sigma(i);
has a maximum as V-s reaches about -30 V because the impurities are m
ost strongly embedded in the film with incoming Ar particles. When -V-
s is over 30 V the more energetic Ar particles contribute to a decreas
e in -sigma(i), through resputtering the impurities. For the Ni/Si sys
tem -sigma(i) only increases monotonically with V-s, mainly owing to t
he peening effect. The anisotropic planar stress sigma(u) which is muc
h smaller in magnitude than sigma(i) is also induced in the film for b
oth systems. The origin of sigma(u) is not understood at present. Thus
, the g-factor varies with V-s,mainly in agreement with the dependence
of sigma(i) on V-s for both systems.