Ri. Todd et al., ANALYSIS OF NEUTRON-DIFFRACTION PEAK BROADENING CAUSED BY INTERNAL-STRESSES IN COMPOSITE-MATERIALS, Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment, 354(1), 1995, pp. 139-144
Neutron diffraction is an essential tool in the study of internal stre
sses in composite materials. In most work only the peak shifts caused
by the related elastic strains are considered, but other valuable info
rmation exists in the form of peak shape changes. The conditions under
which the pure diffraction profile of the composite (i.e. the profile
when all sources of broadening not caused by the residual stresses ar
e removed) represents the probability distribution of the peak shifts
corresponding to the strains are examined. It is shown that in these c
onditions, the pure diffraction profile has no attributes of particle
size broadening (and vice versa), thereby providing a test for the val
idity of results interpreted in this way. The experimental derivation
of measured strain distributions in Al2O3/SiCp composites using neutro
n diffraction is described. No apparent particle size broadening was d
etected, demonstrating the validity of the results, which also satisfi
ed other tests for consistency.