K. Kusaka et al., RESIDUAL-STRESS AND IN-SITU THERMAL-STRESS MEASUREMENT OF ALUMINUM FILM DEPOSITED ON SILICON-WAFER, Thin solid films, 291, 1996, pp. 248-253
Residual stresses in aluminum film deposited on a silicon wafer were m
easured after annealing and quenching. In all cases, residual stresses
were tensile, but slow cooling produced larger stresses than quenchin
g. Residual stresses of slow-cooled samples became relaxed after annea
ling above 300 degrees C. Film passivation by carbon deposition retard
ed the relaxation of residual stress. in-situ X-ray stress measurement
revealed that compressive stresses developed in a heating stage and t
ensile stresses in a cooling stage. From a scanning electron microscop
y observation, it becomes clear that the former contributes to nucleat
ion of hillocks and the latter to void formation and growth.