K. Kusaka et al., EFFECT OF A PLASMA PROTECTION NET ON RESIDUAL-STRESS IN ALN FILMS DEPOSITED BY A MAGNETRON SPUTTERING SYSTEM, Thin solid films, 291, 1996, pp. 260-263
Crystal orientation and residual stress development in AIN films depos
ited on borosilicate glass (the thermal expansion coefficient of which
is nearly equal to that of AIN) substrates were investigated by X-ray
diffraction method. The AIN films were prepared by a conventional pla
nar magnetron sputtering system with a plasma protection net under the
condition of constant substrate temperature and various nitrogen gas
pressures between 0.8 Pa and 13 Pa. We found that the residual stresse
s show the same qualitative tendency against the nitrogen gas pressure
independent of the use of the plasma protection net. Large tensile re
sidual stress was observed at high nitrogen gas pressure and large com
pressive residual stress was observed at low gas pressure. When the pl
asma protection net was used, residual stresses in the AIN him were sh
ifted to the compressive side.