X. Huang et al., EFFECT OF HEAT-TREATMENT ON THE MICROSTRUCTURE OF A METASTABLE BETA-TITANIUM ALLOY, Journal of materials engineering and performance, 3(4), 1994, pp. 560-566
Metastable beta-titanium alloys have improved formability and ductilit
y compared to high-strength alpha- and alpha+beta titanium alloys; thi
s can be attributed to their body-centered cubic structure in the solu
tion-treated condition. In addition, a high strength level can be achi
eved by a simple aging treatment. During manufacturing, components are
subjected to a variety of thermal cycles at temperatures ranging from
650 to 925 degrees C, as well as to cooling rates that vary from air
cooling to furnace cooling. Consequently, various microstructures are
produced that influence the mechanical properties of the products. The
present study was undertaken to characterize the precipitation behavi
or of Timetal 21S at various heat treatment conditions by employing x-
ray diffraction techniques combined with optical and scanning electron
microscopy. It was observed that alpha precipitated preferentially on
the grain boundaries during high-temperature aging (650 degrees C) an
d within the grains during low-temperature aging (400 degrees C). High
-temperature solutioning produced a coarse grain size, and at the same
time enhanced finer a precipitation during aging. The amount of alpha
precipitate attained after the standard aging treatment was about 33%
. Re-solution treatment followed by slow cooling, such as that which o
ccurred during brazing of the alloy, resulted in alpha precipitation d
uring cooling; however, an aging treatment was necessary to precipitat
e an alpha content greater than 20%.