NEW TECHNETIUM(V) AND RHENIUM(V) N-ACETYL ANTHRANILIC ACID (NAA) COMPLEXES

Citation
Rm. Mahfouz et al., NEW TECHNETIUM(V) AND RHENIUM(V) N-ACETYL ANTHRANILIC ACID (NAA) COMPLEXES, Spectroscopy letters, 28(1), 1995, pp. 127-135
Citations number
7
Categorie Soggetti
Spectroscopy
Journal title
ISSN journal
00387010
Volume
28
Issue
1
Year of publication
1995
Pages
127 - 135
Database
ISI
SICI code
0038-7010(1995)28:1<127:NTARNA>2.0.ZU;2-C
Abstract
New N-acetyl anthranilic acid (NAA) -Tc(V) and -Re(V) complexes were p repared by the direct reduction of TcO4- and ReO4- with alkaline and a cidic NaBH4 respectively and in the presence of an excess of ligand. T he complexes were characterized by spectroscopy and elemental analysis . Reversed phase HPLC on Lichrosorb-Rp-18 was used to isolate Tc(V)-NA A complex. Electrophoresis measurements showed them having negative ch arges. The complexes were H-2O soluble.