R. Nowak et al., LOW-LOAD INDENTATION BEHAVIOR OF HFN THIN-FILMS DEPOSITED BY REACTIVERF-SPUTTERING, Journal of materials research, 12(1), 1997, pp. 64-69
Deformation of HfN thin films deposited by the reactive sputtering met
hod on silicon and alumina substrates has been investigated using dept
h-sensing indentation. The experiments performed in a low load range (
2-50 mN) revealed that even extremely shallow indentations were affect
ed by the elastic/plastic response of the substrate. The analysis of t
he shape of the indentation load-depth hysteresis loops and of convent
ional hardness data was supplemented by considerations based on the re
cently proposed energy principle of indentation.