THE PREPARATION OF (BEDO-TTF)(2)CL-CENTER-DOT-3H2O SALT IN BU(4)NHGX(3)-DICHLOROETHANE SYSTEM - SHUBNIKOV-DE HAAS OSCILLATIONS(BU(4)NX+1,2)

Authors
ZHILYAEVA EI TORUNOVA SA LYUBOVSKAYA RN KONOVALIKHIN SV DYACHENKO OA LYUBOVSKII RB PESOTSKII SI
Citation
Ei. Zhilyaeva et al., THE PREPARATION OF (BEDO-TTF)(2)CL-CENTER-DOT-3H2O SALT IN BU(4)NHGX(3)-DICHLOROETHANE SYSTEM - SHUBNIKOV-DE HAAS OSCILLATIONS(BU(4)NX+1,2), Synthetic metals, 83(1), 1996, pp. 7-11
Citations number
18
Categorie Soggetti
Physics, Condensed Matter","Material Science","Polymer Sciences
Journal title
Synthetic metals → ACNP
ISSN journal
03796779
Volume
83
Issue
1
Year of publication
1996
Pages
7 - 11
Database
ISI
SICI code
0379-6779(1996)83:1<7:TPO(SI>2.0.ZU;2-3
Abstract
Electrochemical oxidation of BEDO-TTF (bis(ethylenedioxo)tetrathiafulv alene) in 1,2-dichloroethane in the presence of Bu(4)NHgX(3) + Bu(4)NX (X = I, Br, Cl) as a supporting electrolyte at low current density re sults in the isolation of (BEDO-TTF)(2)Cl . 3H(2)O salt. Its compositi on has been established by a chemical analysis (Cl, C, H), electron pr obe microanalysis and X-ray analysis. The temperature dependence of th e resistance has been studied down to 1.5 K at a pressure up to 30 kba r and at room temperature up to 80 kbar. Field and angular dependences of magnetoresistance have been investigated.