A polysaccharide containing L-rhamnose and L-xylose was isolated from
the lipopolysaccharide extracted from the cell walls of the reference
strain for Stenotrophomonas (Xanthomonas) maltophilia serogroup 010. B
y means of NMR studies and methylation analysis, the repeating unit of
the polymer was identified as a branched tetrasaccharide of the struc
ture shown. [GRAPHICS] itable for use in HF experiments as described i
n this article. The reactor has the advantages of multiple independent
reaction vessels, means to precisely measure liquid KF, means to add
measured volumes of reagents directly to the closed reaction vessels d
uring the course of the solvolysis, and provision for rapid temperatur
e changes and control. A series of experiments exploring the direct tr
ansition from HF solvolysis to acetolysis conditions by the addition o
f acetic acid and acetic anhydride, as an alternative to previously pu
blished solvolysis termination schemes, is also described.