H-1-NMR AS A TOOL FOR THE STRUCTURE ELUCIDATION OF MOENOMYCIN ANTIBIOTICS

Authors
DONNERSTAG A HENNIG L FINDEISEN M WELZEL P HAESSNER R
Citation
A. Donnerstag et al., H-1-NMR AS A TOOL FOR THE STRUCTURE ELUCIDATION OF MOENOMYCIN ANTIBIOTICS, Magnetic resonance in chemistry, 34(12), 1996, pp. 1031-1035
Citations number
17
Categorie Soggetti
Spectroscopy,Chemistry
Journal title
Magnetic resonance in chemistry → ACNP
ISSN journal
07491581
Volume
34
Issue
12
Year of publication
1996
Pages
1031 - 1035
Database
ISI
SICI code
0749-1581(1996)34:12<1031:HAATFT>2.0.ZU;2-E
Abstract
As a consequence of aggregate formation, no H-1 NMR spectra of the amp hiphilic antibiotic moenomycin A have been obtained previously, It was now found that the system moenomycin A-D2O-C6D6 after sonification yi elded highly resolved H-1 NMR spectra, probably due to the formation o f a microemulsion. Similarly resolved spectra were obtained from moeno mycin A in sodium dodecyl sulphate micelles.