Yy. Yang et Rf. Egerton, TESTS OF 2 ALTERNATIVE METHODS FOR MEASURING SPECIMEN THICKNESS IN A TRANSMISSION ELECTRON-MICROSCOPE, Micron, 26(1), 1995, pp. 1-5
Using thin-film standards of Al, Ag, In, Sn, Sb, and Te whose mass-thi
ckness was determined by weighing, we investigated the,accuracy of two
methods of thickness measurement, both of which employ electron energ
y-loss spectroscopy (EELS) in a transmission electron microscope (TEM)
. A method based on the Kramers-Kronig sum rule was found to provide a
n accuracy of better than 15%, given suitable treatment of the low-ene
rgy and surface losses. The log-ratio method, based on measurement of
the total and zero-loss integrals and a parameterized expression for t
he total-inelastic mean free path, yielded more variable accuracy: the
discrepancy with weighed values was less than 5% for Al but amounted
to more than 50% in the case of Se and Te.