U. Vierl et al., ENERGY-DISPERSIVE X-RAY REFLECTIVITY STUDY OF THE MODEL MEMBRANES AT THE AIR-WATER-INTERFACE, Biochimica et biophysica acta. Biomembranes, 1234(1), 1995, pp. 139-143
The results of the first energy-dispersive reflectivity measurements w
ith a (membrane coated) liquid surface are reported. They rely on the
calibration curve measured with pure water and can be done without any
sample or detector movement with a low-intensity, laboratory-based X-
ray generator within less than 1 h. As an illustration, the structural
parameters of a diarachidoylphosphatidylcholine monolayer at the air/
water interface are determined. It is argued that the energy-dispersiv
e detection in combination with the intense synchrotron radiation can
be used for the time-resolved reflectivity measurements on the time-sc
ale of minutes.