Hhk. Xu et al., FRACTURE-RESISTANCE OF SIC-FIBER-REINFORCED SI3N4 COMPOSITES AT AMBIENT AND ELEVATED-TEMPERATURES, Journal of the American Ceramic Society, 78(3), 1995, pp. 698-704
The crack growth behavior in unidirectional SiC-fiber-reinforced Si3N4
-matrix composites fabricated in our laboratories was investigated as
a function of fiber volume fraction and temperature. Both the stress-i
ntensity factor and an energy approach were adopted in the characteriz
ation of the crack growth behavior. Crack resistance increased with cr
ack extension (R-curve or T curve) as a result of bridging effects ass
ociated with the intact fibers. Large-scale bridging was observed, and
was considered in the determination of the R-curves. Temperature and
fiber volume fraction affected the crack propagation behavior. At room
temperature a single crack was initiated at the notch tip; it then br
anched and delaminated upon further loading. In contrast, at 1200 degr
ees C, little crack branching was observed. Increasing fiber volume fr
action increased the degree of crack branching. Temperature and fiber
volume fraction also affected the R-curve behavior. Raising the temper
ature to 1200 degrees C did not significantly degrade the room-tempera
ture R-curve effect. Increasing the fiber volume fraction from 14% to
29% substantially enhanced the toughening effect and the R-curve behav
ior.