Multilayers were prepared on well developed tungsten field-ion microsc
opy (FIM)-tips by subsequent deposition of Pd and Cu with a thickness
of about 20 nm. These specimens were annealed isochronically at temper
atures between 373 and 723 K. Ladder diagrams obtained by the atom-pro
be (AP) from the as-prepared specimens showed an interface between Cu
and Pd layers indicating a depth resolution of about 1 nm. The heat tr
eated specimens revealed clearly an interdiffusion of the species betw
een the layers. In addition, for the first time investigations with th
e three-dimensional tomographic AP were performed on such compounds. P
reliminary results on the as-prepared and annealed specimens are discu
ssed and interdiffusion coefficients of CuPd are compared with data av
ailable from literature.