Jw. Hoehn et al., MICROMECHANICAL TOUGHNESS TEST APPLIED TO NIAL, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 193, 1995, pp. 301-308
A microscratch technique for determining the fracture toughness of bri
ttle intermetallics is presented. Advantages include very small sample
sizes and multiple tests on a single, flat polished surface. The frac
ture toughnesses of single-crystal NiAl in {001}[100], {001}[110], {11
0}[110], and {110}[100] crack orientations were evaluated using this t
echnique. The results of the scratch testing are compared with measure
ments on small compact tension samples. Also, transmission electron mi
croscopy is used to help explain the dislocation character of the resu
lting plastic zones in samples tested. Lastly, a model for determining
the dislocation velocity during nanoindentation is presented to help
understand the ductile-brittle transition temperature of semibrittle m
aterials.