P. Ochmann et H. Vehoff, EXPERIMENTAL INVESTIGATION OF THE FRACTURE-TOUGHNESS OF NIAL BICRYSTALS COMBINED WITH COMPUTER-SIMULATIONS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 193, 1995, pp. 364-370
The dependence on temperature, strain rate and orientation of the frac
ture toughness was measured in NiAl single crystals and bicrystals, an
d the results were compared with the predictions of computer simulatio
ns. The fracture toughness tests were performed in four-point-bending
with NiAl bicrystals notched either parallel or perpendicular to the g
rain boundary. The boundaries of the bicrystals had less than half the
toughness of NiAl single crystals after fracture in liquid nitrogen.
The fracture toughness of specimens notched perpendicular to the grain
boundary was measured as a function of the distance from crack tip to
grain boundary. For small distances the brittle to ductile transition
temperature in bicrystals was lower than in single crystals. With dec
reasing distance, depending on the bicrystal orientation, the toughnes
s either increased or showed a pronounced minimum at intermediate dist
ances. Computer simulations based on dislocation dynamics were perform
ed with the same bicrystal orientations. For the interaction of a disl
ocation pile-up with either a ''soft'' or a ''hard'' grain, similar to
ughness-distance dependences were obtained.