Positron annihilation Dopplerbroadening measurements were carried out
on Cu-Al-Ni based alloys to which Ti, and Ti and Mn was added. The mea
surements reveal a drastic effect in the S-parameter behavior when the
defects anneal out at the transition from martensite to the beta phas
e, When crossing the transition region several times, an increase of t
he S-parameter value is observed. This is interpreted as due to the fo
rmation of dislocations and precipitate-martensite interfaces. In the
alloy with Mn a distinct behavior is observed attributed to vacancy cl
uster formation.