Xh. Gu et al., DEFORMATION MICROMECHANICS IN MODEL CARBON-FIBER-REINFORCED COMPOSITES .1. THE SINGLE-FIBER PULL-OUT TEST, Journal of Materials Science, 30(6), 1995, pp. 1409-1419
Raman spectroscopy has been used to study the deformation micromechani
cs of the single-fibre pull-out test for a carbon fibre/epoxy resin sy
stem using surface-treated and untreated versions of the same type of
PAN-based fibre. It has been possible to determine the detailed strain
distribution along embedded fibres and it has been found that it vari
es with the level of strain in the fibre outside the resin block. The
variation of interfacial shear stress along the fibre/matrix interface
has been determined using the balance of forces equilibrium and this
has been compared with the single values of interfacial shear strength
determined from conventional pull-out analyses. It has been demonstra
ted that it is possible to identify situations where the interface is
well-bonded, partially debonded or fully debonded and also to follow t
he failure mechanisms in detail. It has been found that the level of i
nterfacial adhesion is better for the surface-treated fibre and that,
for the untreated fibre, interfacial failure takes place by the cohesi
ve failure of a weakly-bonded surface skin that appears to be removed
by the surface pretreatment process.