APPLICATION OF HIGH-FIELD PROTON NUCLEAR-MAGNETIC-RESONANCE (H-1-NMR)SPECTROSCOPY FOR THE ANALYSIS OF EXPLOSIVES AND RELATED-COMPOUNDS IN GROUNDWATER SAMPLES - A COMPARISON WITH THE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY (HPLC) METHOD

Citation
A. Preiss et al., APPLICATION OF HIGH-FIELD PROTON NUCLEAR-MAGNETIC-RESONANCE (H-1-NMR)SPECTROSCOPY FOR THE ANALYSIS OF EXPLOSIVES AND RELATED-COMPOUNDS IN GROUNDWATER SAMPLES - A COMPARISON WITH THE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY (HPLC) METHOD, Fresenius' journal of analytical chemistry, 356(7), 1996, pp. 445-451
Citations number
16
Categorie Soggetti
Chemistry Analytical
ISSN journal
09370633
Volume
356
Issue
7
Year of publication
1996
Pages
445 - 451
Database
ISI
SICI code
0937-0633(1996)356:7<445:AOHPN(>2.0.ZU;2-H
Abstract
High-field proton nuclear magnetic resonance (H-1-NMR) spectroscopy wa s applied to the analysis of nitroaromatics and nitramines in ammuniti on waste water. The H-1-chemical shifts data of a variety of reference compounds are presented. Three ground-water samples, taken near the f ormer ammunition plant Elsnig (Saxony), were analysed by high-performa nce liquid chromatography (HPLC) and by proton nuclear magnetic resona nce spectroscopy. The results of HPLC and NMR analyses are compared an d discussed.