X-RAY STUDY AND PHYSICOCHEMICAL ANALYSES OF MAGNESIUM HEXAAQUABROMATE

Authors
LUTOSLAWSKAROGOZ J KAPTURKIEWICZKOWAL E HODOROWICZ SA
Citation
J. Lutoslawskarogoz et al., X-RAY STUDY AND PHYSICOCHEMICAL ANALYSES OF MAGNESIUM HEXAAQUABROMATE, Crystal research and technology, 30(2), 1995, pp. 255-262
Citations number
14
Categorie Soggetti
Crystallography
Journal title
Crystal research and technology → ACNP
ISSN journal
02321300
Volume
30
Issue
2
Year of publication
1995
Pages
255 - 262
Database
ISI
SICI code
0232-1300(1995)30:2<255:XSAPAO>2.0.ZU;2-8
Abstract
Magnesium hexaaquabromate (Mg(H2O)(6)(BrO3)(2)) was obtained and analy sed by means of X-ray powder diffraction, infrared (IR) spectroscopy, and nuclear magnetic resonance (NMR) technique. A thermal analysis of the compound was also carried out. In the temperature range 293-77 K t here was no structural phase transition detected. The space group of t he compound was found to be Pa(3) over bar and the structure of the ma gnesium hexaaquabromate was refined using the Rietveld method.