W. Miszkiewicz et al., RPHPLC METHOD FOR THE ASSAY OF 2 METHYL-4,4-TRIMETHYLENE-4-ISOTHIAZOLIN-3-ONE IN WATER-OIL EMULSIONS, Journal of liquid chromatography, 18(8), 1995, pp. 1583-1589
An HPLC procedure was developed fdr the determination of 2 Methyl 4,5-
trimethylene-4-isothothiazolin-3-one in water-oil emulsions, The analy
tical procedure consists of the extraction in the presence of orthopho
sphoric acid and elution of MTI from Hypersil ODS column with acetonit
rile Solution of H3PO4 - water solution of H3PO4 as a mobile phase.