Supersaturated nanocrystalline Al100-xTix alloys were mechanically all
oyed in a planetary ball mill. For alloys with x = 5 and 10, a mixture
of supersaturated solid solution Al(Ti) and an fee phase coexist whil
e a single supersaturated solid solution Al(Ti) was obtained during me
chanical alloying for x = 15 and 35. With increasing Ti content, from
5 to 35 at%, the grain size of the Al(Ti) solid solution decreased fro
m 40 to 10 nm. The results suggest that fast diffusion along nanocryst
alline grain boundaries is the main alloying process. DSC curves and T
EM observations indicate that solute atom segregation can thermally st
abilize the nanocrystalline solid solutions.