H. Chiu et X. Mao, SHEAR LIGAMENT PHENOMENA IN FE3AL INTERMETALLICS AND MICROMECHANICS OF SHEAR LIGAMENT TOUGHENING, Metallurgical and materials transactions. A, Physical metallurgy andmaterials science, 27(12), 1996, pp. 3817-3825
The environment-assisted cracking behavior of a Fe3Al intermetallic in
an air moisture environment was studied. At room temperature, tensile
ductility was found to be increased with strain rate, from 10.1 pct a
t 1 X 10(-6) s(-1) to 14.3 pct at 2 X 10(-3) s(-1). When tensile tests
were done in heat-treated mineral oil on specimens that have been hea
ted in the oil for 4 hours at 200 degrees C, ductility was found to be
recovered. These results suggest the existence of hydrogen embrittlem
ent. Shear ligaments, which are ligament-like structures connected bet
ween microcracks, were observed on the tensile specimens. They undergo
ductile fracture by shearing and enhance fracture toughness. This tou
ghness enhancement (represented by J(l)) was estimated by a micromecha
nical model. The values of the unknown parameters, which are the avera
ge ligament length (l) over bar, the area fraction V-l, and the work-t
o-fracture tau(1) gamma(1), were obtained from scanning electron micro
scopy (SEM) observation. The total fracture toughness K-c and J(l) wer
e reduced toward a slower strain rate. The experimental fracture tough
ness, K-Q, was found to be increased with strain rate, from 35 MPa roo
t m at 2.54 X 10(-5) mm . s(-1) to 47 MPa root m at 2.54 X 10(-2) mm .
s(-1). The fact that strain rate has a similar effect on K-Q and K-c
verifies the importance of shear ligament in determining fracture toug
hness of the alloy. With the presence of hydrogen, length and work-to-
fracture of the shear ligament were reduced. The toughening effect cau
sed by shear ligament was reduced, and the alloy would behave in a bri
ttle manner.