REACTION OF A GERMYLENE WITH ETHYLENE - A STABLE DIGERMACYCLOBUTANE VIA A GERMIRANE INTERMEDIATE

Citation
H. Ohgaki et al., REACTION OF A GERMYLENE WITH ETHYLENE - A STABLE DIGERMACYCLOBUTANE VIA A GERMIRANE INTERMEDIATE, Organometallics, 14(5), 1995, pp. 2139-2141
Citations number
26
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear
Journal title
ISSN journal
02767333
Volume
14
Issue
5
Year of publication
1995
Pages
2139 - 2141
Database
ISI
SICI code
0276-7333(1995)14:5<2139:ROAGWE>2.0.ZU;2-B
Abstract
1,2-Digermacyclobutane (2) is formed by reaction of a stable germylene (1) with ethylene. The crystal structure of 2 has been, determined by single-crystal X-ray diffraction. The H-1 NMR spectrum of the reactio n, mixture revealed the presence of a germirane having no substituents on the ring carbon.