Hc. Chan et Cc. Yu, AUTOTUNING OF GAIN-SCHEDULED PH CONTROL - AN EXPERIMENTAL-STUDY, Industrial & engineering chemistry research, 34(5), 1995, pp. 1718-1729
pH control is known to be a difficult control problem. In this work, t
he gain-scheduled proportional-integral (PI) controller is used to ove
rcome process nonlinearity. Using the gain-scheduled PI controller the
nonlinear control problem becomes the identification of the titration
curve and the design of the PI controller. With necessary instrumenta
tion and appropriate model parameterization, the titration curve can b
e found in a robust manner. Autotune identification is employed to est
imate the titration curve first and goes on to find the nominal tuning
constants. This is the gain-scheduled autotune identification (g-ATV)
procedure. The g-ATV procedure is tested in a laboratory scale pH neu
tralization system. The results show that robust estimation of the tit
ration curve can be achieved from continuous cycling. Furthermore, rel
iable and effective nonlinear pH control can be obtained in a realisti
c operating condition as shown in this experimental study.