LIQUID-CHROMATOGRAPHIC DETERMINATION OF BROMIDE ION IN CEREALS, FRUIT, VEGETABLES, AND BLOOD WITH A SILVER ELECTRODE IN AN ELECTROCHEMICAL DETECTOR SYSTEM

Citation
B. Lindgren et al., LIQUID-CHROMATOGRAPHIC DETERMINATION OF BROMIDE ION IN CEREALS, FRUIT, VEGETABLES, AND BLOOD WITH A SILVER ELECTRODE IN AN ELECTROCHEMICAL DETECTOR SYSTEM, Journal of AOAC International, 78(3), 1995, pp. 841-845
Citations number
14
Categorie Soggetti
Chemistry Analytical
ISSN journal
10603271
Volume
78
Issue
3
Year of publication
1995
Pages
841 - 845
Database
ISI
SICI code
1060-3271(1995)78:3<841:LDOBII>2.0.ZU;2-R
Abstract
A method is presented for rapid determination of bromide ion in commod ities and blood by paired-ion liquid chromatography with electrochemic al detection, The method involves extraction of samples with water and filtration, Blood is passed through a Sep-Pak C-18 minicolumn, Recove ries are usually close to 100%, with satisfactory precision. The detec tion limit is 1 mg/kg, The method needs little labor and uses no noxio us solvents or reagents.