Statistically designed experiments have been made using partial carbox
ymethylated cotton fabric. The effects of three reaction parameters (c
oncentrations of sodium hydroxide and monochloroacetic acid and time p
eriod) on wet pickup and carboxyl content are presented using polynomi
al models. Monochloroacetic acid concentration seems to be the leading
factor among the parameters investigated. Poor reproducibility of the
drying process could be one possible barrier to industrial applicatio
ns of carboxymethylation.