D. Benda et J. Snuparek, INVESTIGATION OF THE KINETICS OF DISPERSION POLYMERIZATION BY MEANS OF A DILATOMETER OF NEW DESIGN - ROTARY DILATOMETER, Journal of dispersion science and technology, 16(3-4), 1995, pp. 197-203
An instrument for the measurement of the kinetics of dispersion polyme
risation reactions has been developed. The main part of the instrument
consists of a glass dilatometer of a new design which rotates along t
he vertical axis. The direction of rotation changes in short intervals
. Stirring inside the dilatometer occurs through the action of baffles
and the inertia forces of the rotating liquid. The said dilatometer e
xcels in simplicity, correct function, easy cleaning and perfect react
ion heat transfer, It was rested out by performing measurements of the
kinetics of acrylamide polymerisation in inverse emulsion.