Distillation is the most important separation technique for the fracti
onation of oleochemical products like fatty acids, fatty alcohols and
esters. The demand for higher purities and yields has influenced stric
tly the development of this technology during the last 10 years. An up
to date overview is given for the practical use of distillation and r
ectification equipment in the oleochemical industry. Also, aspects of
new rectification sequences, of side stream columns or control concept
s, of safety and of energy savings are discussed. It is expected that
combinations with other unit operations, improvements of batch process
es, new methods of process control will be the main subject of process
development in the next future.