O-Methyloduline and N-demethylmasonine, two so far unknown Amaryllidac
eae alkaloids, have been found in bulbs of Narcissus pseudonarcissus.
Their structures were established by NMR spectroscopy (COLOC and NOE e
xperiments). Complete spectral data for oduline and masonine are also
given. It is shown, that O-methyloduline is not an artefact of plant e
xtraction with methanol.