H. Mahfuz et al., FRACTURE AND FLEXURAL CHARACTERIZATION OF SICW SIC COMPOSITES AT ROOMAND ELEVATED-TEMPERATURES/, Journal of Materials Science, 30(9), 1995, pp. 2406-2411
The fracture and flexural behaviour of monolithic SiC and SiC-whisker
reinforced SiC composites (SiCwSiC) has been investigated at room and
elevated temperatures, Flexure and fracture tests were conducted in a
four-point beam configuration at 23 degrees C, 800 degrees C and 1200
degrees C to study the effects of whisker reinforcements especially in
respect of mechanical and thermal stability at high energy environmen
ts. Flexural strengths and fracture toughness data within the test tem
perature range are presented in graphical as well as in Weibull form,
and experimental observations are analysed and discussed, Increase in
flexural strength as well as in fracture toughness has been observed w
ith the whisker reinforcement. However, it was found that the trend di
scontinues after a certain range of temperature. Post-failure analyses
have been performed with the scanning electron microscope (SEM). Form
ation of glass phase has been observed at the whisker/matrix interface
and the crack growth was found to be shifting from intergranular to t
ransgranular with the rise in temperature. Effects of whisker reinforc
ement and the degradation of flexural and fracture properties at eleva
ted temperature are investigated. Ultrasonic velocity measurements hav
e been performed through the thickness of the untested as well as frac
tured specimen, and the variation in the sonic wave velocity is discus
sed in this paper.