F. Smektala et M. Matecki, DETERMINATION OF ZBLAN GLASS NUCLEATION AND CRYSTALLIZATION CURVES FROM DSC EXPERIMENTS, European journal of solid state and inorganic chemistry, 32(3), 1995, pp. 245-250
A method allowing the determination of nucleation and crystallization
rate curves of fluorozirconate glass (ZBLAN) from differential scannin
g calorimeter experiments (DSC) is described. Starting nucleation and
crystallization temperatures are found to be respectively 260 and 330
degrees C, while the temperatures of the maximum nucleation rate and c
rystallization rate are located around 300 and 380 degrees C.