Ky. Shue et Jw. Yeh, THE CHARACTERIZATION OF THE AL-12 WT PCT SI FLAKE POWDER PRODUCED BY A DOUBLE-DISK PROCESS, Metallurgical and materials transactions. A, Physical metallurgy andmaterials science, 26(6), 1995, pp. 1571-1581
A double-disk (DD) process was developed in this study for producing h
ighly elongated flakes which are very promising for application as a f
iller for conductive composites with a plastic matrix. The Al-12Si all
oy was selected as the experimental alloy in view of its high stiffnes
s, strength, and integrity which are beneficial for retaining its high
aspect ratio during the fabrication of the composites. Various operat
ional parameters, i.e., pouring temperature and the rotational speeds
of upper disk and quenching disk, were monitored in the powder product
ion to reveal their effects on the size distribution and morphology of
flakes. The flake formation mechanism was also investigated. Experime
ntal results indicate that the broad size distribution of the flakes p
roduced by the double-disk process rises from the splat-quenching effe
ct and the formation of interlinked flakes and whisker-shaped flakes.
The mean particle size (or mean flake width) increases with a decreasi
ng rotational speed of centrifugal disk or quenching disk speed, but i
s little influenced by pouring temperature. The length-to-width ratio
of flakes varies with the rotational speed of quenching disk but inver
sely with pouring temperature, centrifugal disk speed, and flake width
. The thickness varies inversely with all of these variables. The aspe
ct ratio varies with pouring temperature, rotational speed of quenchin
g disk, and flake width, but varies inversely with centrifugal disk sp
eed. All of these variations might be accounted for by considering the
solidification rate and dragging rate. Based on these two rates, theo
retical relationships for length-to-width ratio, thickness, and aspect
ratio as a function of various metallurgical factors are derived and
correlate sufficiently with the trends of experimental data.