A new method to produce novel composite materials based on the use of
aerogels as a starting material is described. Using chemical vapor inf
iltration, a variety of solid materials were thermally deposited into
the open pore structure of aerogel. The resulting materials possess ne
w and unusual properties including photoluminescence, magnetism and al
tered optical properties. An important characteristic of this preparat
ion process is the very small size of the deposits that gives rise to
new behaviors. Silicon deposits exhibit photoluminescence, indicating
quantum confinement. Two or more phases may be deposited simultaneousl
y and one or both chemically or thermally reacted to produce new struc
tures.