A new compound, NdBa2Ca3Sr4Cu5OX, has been synthesised using the conve
ntional solid state reaction technique. The material was characterised
by powder XRD, electrical resistivity, ac susceptibility and dc magne
tisation studies. The results of powder X-ray diffraction show that th
e structure is pseudo orthorhombic, having unit cell dimensions a = 5.
47 Angstrom, b = 5.46 Angstrom and c = 14.58 Angstrom. Magnetisation s
tudies on a SQUID magnetometer showed a superconducting transition at
52 K. This was confirmed by the measurements of electrical resistance
and ac susceptibility of this sample, which also showed superconductiv
ity at 52 K. Details of preparation and characterisation are discussed
.