F. Katzenberg et al., A CROSS-SECTIONAL PREPARATION METHOD FOR TEM AND AFM INVESTIGATIONS ON LAYERED POLYMER INTERFACES, Polymer bulletin, 35(1-2), 1995, pp. 195-200
The epitaxial crystallization of polyethylene (PE) on uniaxially orien
ted isotactic polypropylene (iPP) has been investigated by transmissio
n electron microscopy (TEM) and atomic force microscopy (AFM). The cro
ss-sectional morphology of the epitaxial interfaces of multi-layered s
amples prepared by a new preparation method has been observed with vie
w direction parallel to the epitaxial interfaces. It is found that fai
rly oriented PE lamellae grow perpendicular to the iPP layers with nuc
leation initiation on the iPP surfaces.