ELECTROKINETIC CHROMATOGRAPHY OF DITERPENOID ALKALOIDS FROM ACONITUM-SINOMONTANUM NAKAI

Citation
Lg. Song et al., ELECTROKINETIC CHROMATOGRAPHY OF DITERPENOID ALKALOIDS FROM ACONITUM-SINOMONTANUM NAKAI, The Journal of microcolumn separations, 7(2), 1995, pp. 123-126
Citations number
32
Categorie Soggetti
Chemistry Analytical
ISSN journal
10407685
Volume
7
Issue
2
Year of publication
1995
Pages
123 - 126
Database
ISI
SICI code
1040-7685(1995)7:2<123:ECODAF>2.0.ZU;2-W
Abstract
The separation of a hydrophobic mixture of diterpenoid alkaloids from Aconitum sinomontanum Nakai was studied using various modes of electro kinetic chromatography (EKC), such as SDS micellar EKC, methanol or N, N-dimethylformamide modified micellar EKC, beta-cyclodextrin modified micellar EKC, mixed micellar EKC with SDS and PEG 400 monolaurate, and microemulsion EKC with SDS, n-octane and n-butanol. Mixed micellar EK C was found to be the most preferred approach.