SYNTHESIS AND STRUCTURE OF YL-2,4,8,10-TETRAAZABICYCLO[4.4.0]DECANE-3,9-DIONE

Authors
DEKAPRILEVICH MO KRAVCHENKO AN KHMELNITSKII LI LEBEDEV OV STRUCHKOV YT STRELENKO YA
Citation
Mo. Dekaprilevich et al., SYNTHESIS AND STRUCTURE OF YL-2,4,8,10-TETRAAZABICYCLO[4.4.0]DECANE-3,9-DIONE, Russian chemical bulletin, 44(1), 1995, pp. 131-133
Citations number
6
Categorie Soggetti
Chemistry
Journal title
Russian chemical bulletin → ACNP
ISSN journal
10665285
Volume
44
Issue
1
Year of publication
1995
Pages
131 - 133
Database
ISI
SICI code
1066-5285(1995)44:1<131:SASOY>2.0.ZU;2-V
Abstract
yl-2,4,8,10-tetraazabicyclo[4.4.0]decane-3,9-dione a regioisomer of th e previously known yl-2,4,8,10-tetraazabicyclo[4.4.0]decane-3,9-dione has been synthesized, and its structure has been established by X-ray diffraction analysis. The bicyclic system of this molecule is formed b y two heterocycles cis-annelated through the C(1)-C(6) bond. The relat ive configurations of the asymmetric centers are S for C(5), and R for C(7). In the monohydrate crystal studied, the molecules are linked by O...H-O-W and O...H-N type H-bonds forming a three-dimensional framew ork.