Ih. Song et al., IN-SITU TOTAL-ELECTRON-YIELD SULFUR K-EDGE XAFS MEASUREMENTS DURING EXPOSURE OF COPPER TO AN SO2-CONTAINING HUMID ATMOSPHERE, Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment, 360(3), 1995, pp. 634-641
A total-electron-yield (TEY) detector was designed and constructed for
in situ X-ray absorption fine structure (XAFS) measurements of the su
lfur-containing species formed during exposure of copper to a humid at
mosphere containing SO2. Using the detector, gas phase XAFS spectra we
re also collected for both dry and humid SO2 atmospheres. This work pr
esents the experimental technique and examples of the sulfur K-edge sp
ectra collected during the study.