THE PREPARATION OF HIGH-PURITY (H2S)-S-35

Authors
COLLINS CD BELL JNB
Citation
Cd. Collins et Jnb. Bell, THE PREPARATION OF HIGH-PURITY (H2S)-S-35, Journal of labelled compounds & radiopharmaceuticals, 34(11), 1994, pp. 1117-1119
Citations number
4
Categorie Soggetti
Chemistry Analytical","Pharmacology & Pharmacy
Journal title
Journal of labelled compounds & radiopharmaceuticals → ACNP
ISSN journal
03624803
Volume
34
Issue
11
Year of publication
1994
Pages
1117 - 1119
Database
ISI
SICI code
0362-4803(1994)34:11<1117:TPOH(>2.0.ZU;2-D
Abstract
(H2S)-S-35 was synthesised by the reaction of H-2 with elementary [S-3 5] sulphur at 600 degrees C with 100 mg of pumice added as a catalyst. The resulting gas was purified by placing the preparation vessel in a pack of ice. A yield of 46% was produced.