CROSS-LINKING 2,5-DIHYDRO-1H-PYRROL-1-YLOXYL SPIN-LABEL REAGENTS BIFUNCTIONALIZED WITH AZIDOPHTHALIMIDYL AND METHYLTHIOSULFONYLOXY GROUPS

Citation
T. Kalai et al., CROSS-LINKING 2,5-DIHYDRO-1H-PYRROL-1-YLOXYL SPIN-LABEL REAGENTS BIFUNCTIONALIZED WITH AZIDOPHTHALIMIDYL AND METHYLTHIOSULFONYLOXY GROUPS, Synthesis, (10), 1994, pp. 1079-1082
Citations number
18
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
ISSN journal
00397881
Issue
10
Year of publication
1994
Pages
1079 - 1082
Database
ISI
SICI code
0039-7881(1994):10<1079:C2SRB>2.0.ZU;2-#
Abstract
Oxy-Cope and ortho ester Claisen rearrangements of 5- and 6-membered N -oxyl radicals were carried out. The resulting more stable 5-membered bromo derivative 6 was used in the synthesis of bifunctionalized cross linking photo- and thiol-label 12.