L. Enkhjin et Vp. Perelygin, DETERMINATION OF MICROQUANTITIES OF BE IN SAMPLES USING ALPHA-SENSITIVE TRACK ETCH DETECTORS, Radiation measurements, 25(1-4), 1995, pp. 359-362
A new technique of determining Be content in samples using 4.6 divided
by 6 MeV gamma-rays is proposed. This energy range is sufficient to k
nock out the neutron from the Be-9 nucleus and to excite the first 2.9
MeV level of the Be-8 nuclei. 1.5 MeV alpha particles are registered
by means of CR-3S, or cellulose nitrate detectors. Alpha particles pro
duced in the reaction of gamma-rays with Li nuclei which are contained
in samples may cause the background. The latter is excluded by heatin
g of samples before irradiation for Li molecules to be evaporated. B-1
1 nuclei do not produce alpha particles at the energy range of gamma-r
ays presented above. The results obtained in the experiments of determ
ining Be content in natural beryl crystal samples are in good agreemen
t with their known chemical composition. Microparticles containing Ber
yllium were found in soil samples from the Ust-Kamenogorsk are deposit
region, which contains 10(-3) - 10(-4) g/g of Be. The sensitivity of
the method is 10(-6) g/g of Be in solids.