Sm. Clark et al., DEVELOPMENT OF LARGE-VOLUME REACTION CELLS FOR KINETIC-STUDIES USING ENERGY-DISPERSIVE POWDER DIFFRACTION, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 97(1-4), 1995, pp. 98-101
Two novel sample chambers for the energy-dispersive powder diffraction
study of chemical reactions are presented. One for air sensitive samp
les and the other for hydrothermal synthesis. The use of these vessels
is illustrated with data collected during a study of the intercalatio
n of cobaltocene into SnS2.