Wd. Shi et al., MICROSTRUCTURAL INVESTIGATION OF AGGREGATES FORMED FROM AGED SILICA SOLS BY STXM, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 97(1-4), 1995, pp. 202-205
The scanning transmission X-ray microscope at the Daresbury Laboratory
has been used to form direct high-resolution images of gels prepared
from aged silica sols at different pH values. The pH plays an importan
t role in the determination of both the gelation rate and the microstr
uctures observed in the aggregates of the silica gel. The fractal dime
nsion of the structures can be used to study differences between the r
esulting aggregates.