High-purity aluminium (99.996%) has been deformed by cold-rolling to i
ntermediate reductions (50 and 60%). The microstructure has been chara
cterized using transmission electron microscopy (TEM) and the local cr
ystallographic orientations have been analysed by convergent beam elec
tron diffraction (CBED) using a semi-automatic technique. A number of
dislocation configurations such as microbands (MBs), S-bands and lamel
lar boundaries (LBs) have been characterized in terms of crystallograp
hic and macroscopic orientations and morphology. For a large number of
dislocation boundaries, the angle/axis pairs have been calculated and
classified. The microstructural and crystallographic information is c
ombined into orientation images which are related to a framework for t
he microstructural evolution common to medium and high stacking fault
energy f.c.c. polycrystals. This framework consists of a grain subdivi
sion by dislocation boundaries and it is discussed how these boundarie
s evolve especially how intragranular high angle boundaries can form.
The effect of annealing on the deformation microstructure and intragra
nular nucleation is finally discussed.